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Revista de la Sociedad Química del Perú
Print version ISSN 1810-634X
Abstract
CASTRO MANDUJANO, Olivio; PASTOR DE ABRAM, Ana and COLLANTES DIAZ, Ingrit E.. Isolation of the usnic acid and parietin of the Caloplaca saxicola Hoffm. Rev. Soc. Quím. Perú [online]. 2011, vol.77, n.2, pp.152-161. ISSN 1810-634X.
In the present work there was investigated the Caloplaca saxicola (Hoffm.), gathered near Chinchaycocha's lagoon (Carhuamayo - Cerro de Pasco), to an altitude of 4100 msnm. To 240 grams sample, it surrendered to an extraction acetonic for maceration; one separated diverse components of the extract, using the chromatography in column, with the system chloroform - acetone increasing the quantity of acetone; then, the obtained fractions they purified using chromatographic techniques and recrystallizations. Finally, they were elucidated and there decided the structures of the obtained solids, analyzing his spectra of IR, H1NMR, C13NMR, and MS; these are: usnic acid and parietin.
Keywords : Lichen; Caloplaca saxicola; usnic acid; parietin.